N-(2-环戊烯-1-基)-4-甲基苯磺酰胺合成路线 (共 11 条)
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in nitromethane T=80°C; 2 h;
参考文献
Ramesh; Ramulu; Mukkanti; Venkateswarlu
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2904 - 2908
反应条件
Hg(OTf)2 in dichloromethane T=20°C; 0.5 h;
参考文献
Yamamoto, Hirofumi; Ho, Elisabeth; Sasaki, Ikuo; Mitsutake, Mizuho; Takagi, Yuichi; Imagawa, Hiroshi; Nishizawa, Mugio
European Journal of Organic Chemistry, 2011 , # 13 p. 2417 - 2420
反应条件
sec.-butyllithium in diethyl ether; cyclohexane T=-78°C; 4 h;
参考文献
O'Brien, Peter; Rosser, Clare M.; Caine, Darren
Tetrahedron, 2003 , vol. 59, # 49 p. 9779 - 9791
反应条件
copper(II) bis(trifluoromethanesulfonate) in acetonitrile T=20°C; 2.5 h;
参考文献
Kim; Choi; Mang; Lee
Synthetic Communications, 2001 , vol. 31, # 16 p. 2463 - 2469
反应条件
n-butyllithium; potassium tert-butylate; diisopropylamine in hexane; pentane T=20°C;
参考文献
Mordini, Alessandro; Russo, Francesco; Valacchi, Michela; Zani, Lorenzo; Degl'Innocenti, Alessandro; Reginato, Gianna
Tetrahedron, 2002 , vol. 58, # 35 p. 7153 - 7163
反应条件
Co(acacen) in benzene T=75°C; 3 h;
参考文献
Caselli, Alessandro; Gallo, Emma; Ragaini, Fabio; Oppezzo, Alessandro; Cenini, Sergio
Journal of Organometallic Chemistry, 2005 , vol. 690, # 8 SPEC. ISS. p. 2142 - 2148
反应条件
[Cu([2.1.1]-(2,6-pyridinophane)Cl]; Na[B(3,5-(CF3)2C6H3)4] in dichloromethane T=0°C; 0.0333333 h;
参考文献
Vedernikov, Andrei N.; Caulton, Kenneth G.
Organic Letters, 2003 , vol. 5, # 15 p. 2591 - 2594
反应条件
copper(II) bis(trifluoromethanesulfonate) in dichloromethane 60 h; Ambient temperature;
参考文献
Kohmura, Yoshinori; Kawasaki, Ken-Ichi; Katsuki, Tsutomu
Synlett, 1997 , # 12 p. 1456 - 1458
反应条件
1: 88 percent / PhMe3N(1+)*Br3(1-) / acetonitrile; H2O / 16 h / 20 °C 2: 23 percent / sec-butyllithium; TMEDA / cyclohexane; diethyl ether / 4 h / -78 °C View Scheme
参考文献
Mordini, Alessandro; Russo, Francesco; Valacchi, Michela; Zani, Lorenzo; Degl'Innocenti, Alessandro; Reginato, Gianna
Tetrahedron, 2002 , vol. 58, # 35 p. 7153 - 7163
反应条件
1: 88 percent / PhMe3N(1+)*Br3(1-) / acetonitrile; H2O / 16 h / 20 °C 2: 23 percent / sec-butyllithium; TMEDA / cyclohexane; diethyl ether / 4 h / -78 °C View Scheme
参考文献
Mordini, Alessandro; Russo, Francesco; Valacchi, Michela; Zani, Lorenzo; Degl'Innocenti, Alessandro; Reginato, Gianna
Tetrahedron, 2002 , vol. 58, # 35 p. 7153 - 7163