1-(1-丁炔-1-基)-4-甲氧基苯合成路线 (共 3 条)
反应条件
NW(OC(CF3)2Me)3(DME) in toluene T=95°C; 10 h; Inert atmosphere;
参考文献
Geyer, Andrea M.; Gdula, Robyn L.; Wiedner, Eric S.; Johnson, Marc J. A.
Journal of the American Chemical Society, 2007 , vol. 129, # 13 p. 3800 - 3801
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc dibromide in tetrahydrofuran T=60°C; Negishi cross-coupling reaction; 4 h;
参考文献
Zhang, Wei; Kraft, Stefan; Moore, Jeffrey S.
Journal of the American Chemical Society, 2004 , vol. 126, # 1 p. 329 - 335
反应条件
4-nitro-phenol; CH3CH2CMo[N(t-Bu)(3,5-C6H3Me2)]3 in various solvent(s) T=30°C; P=1 Torr; 22 h;
参考文献
Zhang, Wei; Kraft, Stefan; Moore, Jeffrey S.
Journal of the American Chemical Society, 2004 , vol. 126, # 1 p. 329 - 335