1-(4-戊烯-1-基)-1H-吡咯合成路线 （共 5 条）
反应条件
potassium hydride in tetrahydrofuran T=18°C; 16 h;
参考文献
Banwell, Martin G.; Beck, Daniel A.S.; Smith, Jason A.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 2 p. 157 - 159
反应条件
1: 53 percent / Et3N, DMAP / CH2Cl2 2: 92 percent / KOH / dimethylsulfoxide 3: 94 percent / 0.1M HCl / methanol 4: 89 percent / Et3N, DMAP / CH2Cl2 5: 10 Na<Co(dmgh)2Py>, 2) PPTS / 1) MeOH, 2) CHCl3, RT View Scheme
参考文献
Gage, Jennifer L.; Branchaud, Bruce P.
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7007 - 7010
反应条件
1: 92 percent / KOH / dimethylsulfoxide 2: 94 percent / 0.1M HCl / methanol 3: 89 percent / Et3N, DMAP / CH2Cl2 4: 10 Na<Co(dmgh)2Py>, 2) PPTS / 1) MeOH, 2) CHCl3, RT View Scheme
参考文献
Gage, Jennifer L.; Branchaud, Bruce P.
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7007 - 7010
反应条件
1: 61 percent / TsOH*H2O 2: 53 percent / Et3N, DMAP / CH2Cl2 3: 92 percent / KOH / dimethylsulfoxide 4: 94 percent / 0.1M HCl / methanol 5: 89 percent / Et3N, DMAP / CH2Cl2 6: 10 Na<Co(dmgh)2Py>, 2) PPTS / 1) MeOH, 2) CHCl3, RT View Scheme
参考文献
Gage, Jennifer L.; Branchaud, Bruce P.
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7007 - 7010
反应条件
1: 94 percent / 0.1 M HCl / Heating 2: 61 percent / TsOH*H2O 3: 53 percent / Et3N, DMAP / CH2Cl2 4: 92 percent / KOH / dimethylsulfoxide 5: 94 percent / 0.1M HCl / methanol 6: 89 percent / Et3N, DMAP / CH2Cl2 7: 10 Na<Co(dmgh)2Py>, 2) PPTS / 1) MeOH, 2) CHCl3, RT View Scheme
参考文献
Gage, Jennifer L.; Branchaud, Bruce P.
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7007 - 7010
