sodium periodate in methanol 18 h; Ambient temperature;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4546405', constants.ctx, '0')">caesium carbonate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=20&deg;C;&nbsp;2&nbsp;h;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1735581', constants.ctx, '0')">di-tert-butyl peroxide</a> <br />T=120&deg;C;&nbsp;24&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1735581', constants.ctx, '0')">di-tert-butyl peroxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3602276', constants.ctx, '0')">palladium diacetate</a> <br />T=120&deg;C;&nbsp;12&nbsp;h;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> &nbsp;

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1708400', constants.ctx, '0')">2,2'-azo-bisisobutyronitrile</a> <br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342940', constants.ctx, '0')">sodium hydroxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3535005', constants.ctx, '0')">borane</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587191', constants.ctx, '0')">dihydrogen peroxide</a> <br />&nbsp;1.) THF, room temperature, overnight, 2.) toluene, reflux, 27 h;&nbsp;&nbsp;Yield given. Multistep reaction;&nbsp;<br /> &nbsp;