反应条件
1: 90 percent / dimethylsulfoxide / 66 h / 80 °C 2: 90 percent / H2 / 10 percent Pd/BaSO4 / ethyl acetate / 2 h 3: 97 percent / K2CO3 / methanol; H2O / 15 h / Ambient temperature 4: 1) Mg / 2) THF, 1 h, 50 deg C 5: 91 percent / pyridine 6: 1) PI3; 2) LiAlH4 / 1) CS2, room temp., 30 min, ether; 2) THF, 90 min, reflux View Scheme
参考文献
Sucrow, Wolfgang; Nooy, Michael van
Liebigs Annalen der Chemie, 1982 , # 10 p. 1897 - 1906
