1-烯丙基-2,3-二甲氧基苯合成路线 （共 13 条）
反应条件
anschliessendes Erhitzen mit Wasserdampf;
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1937 , vol. <2> 148, p. 95,97
反应条件
1.1: osmium(VIII) oxide; sodium periodate; sodium hydrogencarbonate / methanol; water; toluene / 0.33 h / 20 °C
2.1: methanol; water; toluene / 2 h
3.1: palladium on activated charcoal; hydrogen / methanol / 10 h
4.1: sulfuric acid / 0.25 h / 85 - 90 °C
4.2: 2 h / |Reflux
View Scheme
参考文献
Lahiri, Saswata; Ramarao; Rao, B. Venkateswara; Rao, A.V. Rama; Chorghade, Mukund S.
Organic Process Research and Development, 1999 , vol. 3, # 1 p. 71 - 72
反应条件
trichlorophosphate
1) 10 deg C, 45 min 2) r.t., 120 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Narasimhan, N. S.; Mukhopadhyay, T.; Kusurkar, S. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 546 - 548
