2-[(8-氯辛基)氧基]四氢-2H-吡喃合成路线 (共 7 条)
反应条件
in dimethyl sulfoxide
参考文献
The United States of America as represented by the Secretary of Agriculture
Patent: US4083995 A1, 1978 ;
反应条件
in dimethyl sulfoxide 15 h; Ambient temperature;
参考文献
Kasymzhanova, M.; Abdukakharov, V. S.; Kamaev, F. G.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, # 6 p. 708 - 713
Khimiya Prirodnykh Soedinenii, 1989 , # 6 p. 834 - 840
参考文献
Karpinska; Lewandowska; Grodner
Polish Journal of Chemistry, 2004 , vol. 78, # 7 p. 937 - 942
反应条件
n-butyllithium 1. hexane, THF, 30min; 2. hexametapol, 1h; Yield given. Multistep reaction;
参考文献
Kasymzhanova, M.; Abdukakharov, V. S.; Kamaev, F. G.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, # 6 p. 708 - 713
Khimiya Prirodnykh Soedinenii, 1989 , # 6 p. 834 - 840
反应条件
lithium amide hexamethylphosphoroamide, 1.) 1h, room temperature, 2.) 10 h, 55 deg C; Multistep reaction;
参考文献
Kovalev, B. G.; Matveeva, E. D.; Stan, V. V.; Vovk, G. A.; Yudin, L. G.; Kost, A. N.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1728 - 1733
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2032 - 2038
反应条件
pyridine; lithium amide
Yield given. Multistep reaction;
参考文献
Kasymzhanova, M.; Abdukakharov, V. S.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1992 , vol. 28, # 5 p. 525 - 526
Khimiya Prirodnykh Soedinenii, 1992 , # 5 p. 598 - 599
反应条件
sodium iodide in acetone
72 h; Heating;
参考文献
Descoteaux, Caroline; Leblanc, Valerie; Belanger, Geoffroy; Parent, Sophie; Asselin, Eric; Berube, Gervais
Steroids, 2008 , vol. 73, # 11 p. 1077 - 1089