四(二甲基胺基)锆(IV)合成路线 (共 5 条)
反应条件
in toluene N2-atmosphere; stirring (room temp., 18 h); evapn. (reduced pressure), subliming (80°C, 0.05 mmHg);
参考文献
Diamond, Gary M.; Rodewald, Stephan; Jordan, Richard F.
Organometallics, 1995 , vol. 14, p. 5 - 7
参考文献
Dalton Transactions, , # 3 p. 427 - 428
反应条件
in benzene-d6 treatment of zirconium compd. with 6 equiv. of lithium dimethylamide in benzene-d6 at 60°C for 24 h;
参考文献
Organometallics, , vol. 27, # 11 p. 2399 - 2401
反应条件
in not given byproducts: (CH3)2N;
参考文献
Bar-Haim, Galia; Shach, Romem; Kol, Moshe
Chemical Communications, 1997 , # 2 p. 229 - 230
反应条件
T=200°C; P=1.9952 Torr; 0.00833333 - 0.133333 h;
参考文献
MITSUBISHI MATERIALS CORPORATION
Patent: US2004/210071 A1, 2004 ;
Location in patent: Page 9 ;