二乙基4-甲基-2,6-吡啶二羧酸酯合成路线 （共 4 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; copper(l) chloride in N,N-dimethyl-formamide
T=60°C; Stille Cross Coupling;
参考文献
Hamada, Yoshio; Suzuki, Kenji; Nakanishi, Tomoya; Sarma, Diganta; Ohta, Hiroko; Yamaguchi, Ryoji; Yamasaki, Moe; Hidaka, Koushi; Ishiura, Shoichi; Kiso, Yoshiaki
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 618 - 623
反应条件
1: toluene / Heating
2: HCl / aq. NaOH
3: SOCl2 / ethanol / 7 h / Heating
View Scheme
参考文献
Chavarot, Murielle; Socquet, Stephane; Kotera, Mitsuharu; Lhomme, Jean
Tetrahedron, 1997 , vol. 53, # 40 p. 13749 - 13756
反应条件
1: HCl / aq. NaOH
2: SOCl2 / ethanol / 7 h / Heating
View Scheme
参考文献
Chavarot, Murielle; Socquet, Stephane; Kotera, Mitsuharu; Lhomme, Jean
Tetrahedron, 1997 , vol. 53, # 40 p. 13749 - 13756
反应条件
1: tetrakis(triphenylphosphine) palladium(0) / toluene
2: potassium carbonate; tris-(dibenzylideneacetone)dipalladium(0); copper(l) chloride / N,N-dimethyl-formamide / 60 °C
View Scheme
参考文献
Hamada, Yoshio; Suzuki, Kenji; Nakanishi, Tomoya; Sarma, Diganta; Ohta, Hiroko; Yamaguchi, Ryoji; Yamasaki, Moe; Hidaka, Koushi; Ishiura, Shoichi; Kiso, Yoshiaki
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 2 p. 618 - 623
