N-甲基苯并[d]噁唑-2-胺合成路线 (共 8 条)
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; acetic acid in water; 1,2-dichloro-ethane T=90°C; 12 h; Green chemistry;
参考文献
Wang, Rui; Liu, Hong; Yue, Liang; Zhang, Xiao-Ke; Tan, Qiu-Yuan; Pan, Ruo-Lin
Tetrahedron Letters, 2014 , vol. 55, # 14 p. 2233 - 2237
反应条件
ozone in dichloromethane T=25°C;
参考文献
Saladino, Raffaele; Crestini, Claudia; Occhionero, Francesca; Nicoletti, Rosario
Synthetic Communications, 1996 , vol. 26, # 17 p. 3241 - 3251
反应条件
Ni-PO in acetonitrile 5 h; Ambient temperature;
参考文献
Ocura, Haruo; Mineo, Satoshi; Nakagawa, Kunio
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1518 - 1524
反应条件
in methanol; water T=125°C;
参考文献
Ogura,H. et al.
Chemical and Pharmaceutical Bulletin, 1970 , vol. 18, p. 2204 - 2207
反应条件
1: 52 percent / benzene / 1 h / Heating 2: 65 percent / Ni-PO / acetonitrile / 5 h / Ambient temperature View Scheme
参考文献
Ocura, Haruo; Mineo, Satoshi; Nakagawa, Kunio
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1518 - 1524
反应条件
in ethanol; water 20 h; Heating;
参考文献
Hetzheim; Schlaak; Kerstan
Pharmazie, 1987 , vol. 42, # 2 p. 80 - 82
反应条件
1: NaHS 2: 100 °C View Scheme
参考文献
Desai et al.
Journal of the Chemical Society, 1934 , p. 1186,1190
反应条件
1: With nitric acid
T=20°C; 8 h;
2: With sodium hydrogencarbonate in water
T=0°C;
参考文献
SmithKline Beecham p.l.c.
Patent: US6699879 B1, 2004 ;
Location in patent: Page/Page column 24-25 ;