4-氯甲基-3,5-二甲基异噁唑合成路线 (共 13 条)
反应条件
hydrogenchloride; zinc(II) chloride in acetic acid T=35 - 40°C; 3 h;
参考文献
Synthesis, , # 8 p. 1104 - 1106
反应条件
hydrogenchloride; formaldehyd in water T=70°C;
参考文献
WO2006/32384 A1, ;
Page/Page column 70 ;
WO 2006/032384 A1
反应条件
thionyl chloride in dichloromethane 1.5 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 6 p. 1557 - 1560
反应条件
hydrogenchloride; 1,2-dichloro-ethane; zinc(II) chloride
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 2736,2743; engl. Ausg. S. 2762, 2768
反应条件
in xylene 22.5 h; Heating;
参考文献
Maestro, Alicia; Banez, Jose M.; Lopez, Juan A.; Romero-Avila, Maria Cristina
Synthesis, 1998 , # 8 p. 1104 - 1106
反应条件
1: toluene / Heating 2: NaH, DMSO View Scheme
参考文献
Scott; Saucy
The Journal of organic chemistry, 1972 , vol. 37, # 10 p. 1652 - 1658
参考文献
Imperial Chemical Industries PLC; National Research Development Corporation
Patent: US5089499 A1, 1992 ;
参考文献
Kotschetkow et al.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 2736,2743; engl. Ausg. S. 2762, 2768
反应条件
potassium dichromate; sulfuric acid
参考文献
Kotschetkow et al.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 2736,2743; engl. Ausg. S. 2762, 2768
反应条件
methanol; samarium diiodide in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Natale, Nicholas R.
Tetrahedron Letters, 1982 , vol. 23, # 48 p. 5009 - 5012