2-碘-4-[3-(三氟甲基)-3H-二氮杂环丙烯-3-基]苄醇合成路线 (共 2 条)
反应条件
thallium(III) trifluoromethanesulfonate; trifluoroacetic acid; sodium iodide 1.) 80 deg C, 2 h, 2.) RT, 45 min; Yield given. Multistep reaction;
参考文献
Weber, Thomas; Brunner, Josef
Journal of the American Chemical Society, 1995 , vol. 117, # 11 p. 3084 - 3095
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol T=20°C; Catalytic hydrogenation; P=760.051 Torr;
参考文献
Journal of Organic Chemistry, , vol. 65, # 21 p. 7183 - 7186