2,7-二溴-9,9-二乙基芴合成路线 （共 7 条）
反应条件
tetrabutylammomium bromide; potassium hydroxide
参考文献
Feng, Xuli; Lv, Fengting; Liu, Libing; Yang, Qiong; Wang, Shu; Bazan, Guillermo C.
Advanced Materials, 2012 , vol. 24, # 40 p. 5428 - 5432
反应条件
bromine; iodine in dichloromethane T=20°C; Bromination; 24 h;
参考文献
Tsuie, Barbara; Reddinger, Jerry L.; Sotzing, Gregory A.; Soloducho, Jadwiga; Katritzky, Alan R.; Reynolds, John R.
Journal of Materials Chemistry, 1999 , vol. 9, # 9 p. 2189 - 2200
反应条件
1: KI; KOH / dimethylsulfoxide 2: Br2 / dimethylformamide View Scheme
参考文献
Molecular Crystals and Liquid Crystals, , vol. 444, p. 121 - 128
反应条件
potassium hydroxide in dimethyl sulfoxide
参考文献
Organic Electronics: physics, materials, applications, , vol. 12, # 1 p. 125 - 135
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / Cooling with ethanol-dry ice 1.2: 2.5 h 1.3: 5 °C 2.1: dimethyl sulfoxide / 0.75 h / 195 °C View Scheme
参考文献
Zhang, Bingguang; Li, Yunjing; Liu, Rui; Pritchett, Timothy M.; Azenkeng, Alexander; Ugrinov, Angel; Haley, Joy E.; Li, Zhongjing; Hoffmann, Mark R.; Sun, Wenfang
Chemistry - A European Journal, 2012 , vol. 18, # 15 p. 4593 - 4606
反应条件
1.1: n-BuLi / diethyl ether / -78 °C
1.2: diethyl ether
2.1: PBr3 / tetrahydrofuran
View Scheme
参考文献
Kay, Kwang-Yol; Kim, Jung-Hoon; Kim, Sun-Ho; Park, Ho-Cheol; Park, Jong-Wook
Molecular Crystals and Liquid Crystals, 2006 , vol. 444, p. 121 - 128
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; water; toluene
T=90°C; 24 h; Inert atmosphere;
参考文献
Pu, Yong-Jin; Higashidate, Makoto; Nakayama, Ken-Ichi; Kido, Junji
Journal of Materials Chemistry, 2008 , vol. 18, # 35 p. 4183 - 4188
