1: 86 percent / propan-2-ol / 6 h / 80 °C 2: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h View Scheme
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
1: 86 percent / propan-2-ol / 6 h / 80 °C 2: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h 3: 48 percent / 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide, N-ethylmorpholine / tetrahydrofuran / 64 h / Ambient temperature 4: H2 / 10percent Pd/C / ethanol / 16 h 5: 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide, N-ethylmorpholine / tetrahydrofuran / 16 h / Ambient temperature View Scheme
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
1: 86 percent / propan-2-ol / 6 h / 80 °C
2: 100 percent / H2 / 10percent Pd/C / ethanol / 24 h
3: 48 percent / 1-hydroxybenzotriazole hydrate, dicyclohexylcarbodiimide, N-ethylmorpholine / tetrahydrofuran / 64 h / Ambient temperature
View Scheme
参考文献
Parkes, Kevin E. B.; Bushnell, David J.; Crackett, Peter H.; Dunsdon, Stephen J.; Freeman, Andrew C.; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3656 - 3664
Sham, Hing L.; Betebenner, David A.; Zhao, Chen; Wideburg, Norman E.; Saldivar, Ayda; et al.
Journal of the Chemical Society, Chemical Communications, 1993 , # 13 p. 1052 - 1053
