2-[(p-甲基-alpha-苯基苄基)氧基]乙基(二甲基)胺合成路线 （共 7 条）
反应条件
in ethanol; water T=20°C; 72 h;
参考文献
Mueller, Paul; Nury, Patrice; Bernardinelli, Gerald
European Journal of Organic Chemistry, 2001 , # 21 p. 4137 - 4147
反应条件
sodium hydride in toluene 5 h; Heating;
参考文献
Wolf, Cornelia; Schunack, Walter
Archiv der Pharmazie, 1996 , vol. 329, # 2 p. 87 - 94
反应条件
1: 89 percent / BF3*OEt2; sparteine / diethyl ether / -78 °C 2: PPh3; imidazole; I2 / diethyl ether; acetonitrile / 0.5 h / 20 °C 3: 94 percent / ethanol; H2O / 72 h / 20 °C View Scheme
参考文献
Mueller, Paul; Nury, Patrice; Bernardinelli, Gerald
European Journal of Organic Chemistry, 2001 , # 21 p. 4137 - 4147
反应条件
1: 89 percent / BF3*OEt2; sparteine / diethyl ether / -78 °C 2: PPh3; imidazole; I2 / diethyl ether; acetonitrile / 0.5 h / 20 °C 3: 94 percent / ethanol; H2O / 72 h / 20 °C View Scheme
参考文献
Mueller, Paul; Nury, Patrice; Bernardinelli, Gerald
European Journal of Organic Chemistry, 2001 , # 21 p. 4137 - 4147
反应条件
1: PPh3; imidazole; I2 / diethyl ether; acetonitrile / 0.5 h / 20 °C 2: 94 percent / ethanol; H2O / 72 h / 20 °C View Scheme
参考文献
Mueller, Paul; Nury, Patrice; Bernardinelli, Gerald
European Journal of Organic Chemistry, 2001 , # 21 p. 4137 - 4147
反应条件
1,2-dichloro-benzene T=160°C;
参考文献
Parke Davis and Co.
Patent: US2527962 , 1947 ;
反应条件
in 1,2-dichloro-benzene Heating;
参考文献
Harms,A.F.; Nauta,W.T.
J. Med. Chem., 1960 , vol. 2, p. 57 - 77
