您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
198063-87-5
合成路线
（共 7 条）
198064-81-2
→
反应条件
198063-87-5
反应条件
pyridine; trichlorophosphate T=125°C; 1.5 h;
参考文献
Maekawa, Tsuyoshi; Sakai, Nozomu; Tawada, Hiroyuki; Murase, Katsuhito; Hazama, Masatoshi; Sugiyama, Yasuo; Momose
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 5 p. 565 - 573
1501-26-4
4-氯甲酰基丁酸甲酯
→
反应条件
198063-87-5
反应条件
1: 91 percent / AlCl3 / 2 h / 20 °C 2: 88 percent / Br2 / CH2Cl2 / 20 °C 3: HCO2Na / methanol / 12 h / Heating 4: 61.2 g / pyridine / tetrahydrofuran / 1 h / 20 °C 5: 79 percent / NH4OAc; AcOH / 2 h / Heating 6: 73 percent / POCl3; pyridine / 1.5 h / 125 °C View Scheme
参考文献
Maekawa, Tsuyoshi; Sakai, Nozomu; Tawada, Hiroyuki; Murase, Katsuhito; Hazama, Masatoshi; Sugiyama, Yasuo; Momose
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 5 p. 565 - 573
71354-29-5
→
反应条件
198063-87-5
反应条件
1: 88 percent / Br2 / CH2Cl2 / 20 °C 2: HCO2Na / methanol / 12 h / Heating 3: 61.2 g / pyridine / tetrahydrofuran / 1 h / 20 °C 4: 79 percent / NH4OAc; AcOH / 2 h / Heating 5: 73 percent / POCl3; pyridine / 1.5 h / 125 °C View Scheme
参考文献
Maekawa, Tsuyoshi; Sakai, Nozomu; Tawada, Hiroyuki; Murase, Katsuhito; Hazama, Masatoshi; Sugiyama, Yasuo; Momose
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 5 p. 565 - 573
108-90-7
氯苯
→
反应条件
198063-87-5
反应条件
1: 91 percent / AlCl3 / 2 h / 20 °C 2: 88 percent / Br2 / CH2Cl2 / 20 °C 3: HCO2Na / methanol / 12 h / Heating 4: 61.2 g / pyridine / tetrahydrofuran / 1 h / 20 °C 5: 79 percent / NH4OAc; AcOH / 2 h / Heating 6: 73 percent / POCl3; pyridine / 1.5 h / 125 °C View Scheme
参考文献
Maekawa, Tsuyoshi; Sakai, Nozomu; Tawada, Hiroyuki; Murase, Katsuhito; Hazama, Masatoshi; Sugiyama, Yasuo; Momose
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 5 p. 565 - 573
198064-79-8
→
反应条件
198063-87-5
反应条件
1: 61.2 g / pyridine / tetrahydrofuran / 1 h / 20 °C 2: 79 percent / NH4OAc; AcOH / 2 h / Heating 3: 73 percent / POCl3; pyridine / 1.5 h / 125 °C View Scheme
参考文献
Maekawa, Tsuyoshi; Sakai, Nozomu; Tawada, Hiroyuki; Murase, Katsuhito; Hazama, Masatoshi; Sugiyama, Yasuo; Momose
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 5 p. 565 - 573
89150-43-6
→
反应条件
198063-87-5
反应条件
1: HCO2Na / methanol / 12 h / Heating 2: 61.2 g / pyridine / tetrahydrofuran / 1 h / 20 °C 3: 79 percent / NH4OAc; AcOH / 2 h / Heating 4: 73 percent / POCl3; pyridine / 1.5 h / 125 °C View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 51, # 5 p. 565 - 573
198064-80-1
→
反应条件
198063-87-5
反应条件
1: 79 percent / NH4OAc; AcOH / 2 h / Heating 2: 73 percent / POCl3; pyridine / 1.5 h / 125 °C View Scheme
参考文献
Maekawa, Tsuyoshi; Sakai, Nozomu; Tawada, Hiroyuki; Murase, Katsuhito; Hazama, Masatoshi; Sugiyama, Yasuo; Momose
Chemical and pharmaceutical bulletin, 2003 , vol. 51, # 5 p. 565 - 573
