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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1981-50-6
合成路线
（共 11 条）
10269-71-3
→
反应条件
1981-50-6
反应条件
hydrogen; nickel in pyridine; methanol Catalytic hydrogenation; 0.5 h;
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
3452-09-3
1-壬炔
→
反应条件
1981-50-6
反应条件
1: LiNH2 / dioxane / 3.5 h / Heating 2: 95 percent / dioxane / 2 h / Heating 3: 88 percent / ethanol / 5 h / Heating 4: 66 percent / aq. NaOH / ethanol / 10 h / Heating 5: 81 percent / H2 / Raney nickel / methanol; pyridine / 0.5 h View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
51526-03-5
1,7-二碘庚烷
→
反应条件
1981-50-6
反应条件
1: 95 percent / dioxane / 2 h / Heating 2: 88 percent / ethanol / 5 h / Heating 3: 66 percent / aq. NaOH / ethanol / 10 h / Heating 4: 81 percent / H2 / Raney nickel / methanol; pyridine / 0.5 h View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
3330-35-6
→
反应条件
1981-50-6
反应条件
1: 88 percent / ethanol / 5 h / Heating 2: 66 percent / aq. NaOH / ethanol / 10 h / Heating 3: 81 percent / H2 / Raney nickel / methanol; pyridine / 0.5 h View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
4549-31-9
1,7-二溴庚烷
→
反应条件
1981-50-6
反应条件
1: 96 percent / NaI / acetone / 3 h / Heating 2: 95 percent / dioxane / 2 h / Heating 3: 88 percent / ethanol / 5 h / Heating 4: 66 percent / aq. NaOH / ethanol / 10 h / Heating 5: 81 percent / H2 / Raney nickel / methanol; pyridine / 0.5 h View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
60765-09-5
→
反应条件
1981-50-6
反应条件
1: 95 percent / dioxane / 2 h / Heating 2: 88 percent / ethanol / 5 h / Heating 3: 66 percent / aq. NaOH / ethanol / 10 h / Heating 4: 81 percent / H2 / Raney nickel / methanol; pyridine / 0.5 h View Scheme
参考文献
Avis; Boulanger; Belanger
Journal of Chemical Ecology, 2000 , vol. 26, # 4 p. 987 - 1000
99669-96-2
→
反应条件
1981-50-6
反应条件
1: (i) LiNH2, dioxane, (ii) /BRN= 1697887/ 2: (i) aq. EtOH, (ii) NaOH 3: H2 / Raney-Ni / methanol; pyridine View Scheme
参考文献
Grimmer,G.; Kracht,J.
Chemische Berichte, 1963 , vol. 96, p. 3370 - 3373
14101-91-8
→
反应条件
1981-50-6
反应条件
water; sodium hydroxide in methanol 1 h; Heating;
参考文献
Ando, Akinori; Ogawa, Jun; Kishino, Shigenobu; Ito, Taiyo; Shirasaka, Norifumi; Sakuradani, Eiji; Yokozeki, Kenzo; Shimizu, Sakayu
JAOCS, Journal of the American Oil Chemists' Society, 2009 , vol. 86, # 3 p. 227 - 233
55362-80-6
9-溴-1-壬醇
→
反应条件
1981-50-6
反应条件
1.1: acetonitrile / 48 h / |Inert atmosphere; |Reflux 2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 20 °C / |Inert atmosphere 2.2: 1 h / -78 °C / |Inert atmosphere 3.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / water; acetonitrile / 12 h / 20 °C View Scheme
参考文献
Bruns, Hilke; Thiel, Verena; Voget, Sonja; Patzelt, Diana; Daniel, Rolf; Wagner-Doebler, Irene; Schulz, Stefan
Chemistry and Biodiversity, 2013 , vol. 10, # 9 p. 1559 - 1573
73945-70-7
→
反应条件
1981-50-6
反应条件
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 20 °C / |Inert atmosphere 1.2: 1 h / -78 °C / |Inert atmosphere 2.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / water; acetonitrile / 12 h / 20 °C View Scheme
参考文献
Bruns, Hilke; Thiel, Verena; Voget, Sonja; Patzelt, Diana; Daniel, Rolf; Wagner-Doebler, Irene; Schulz, Stefan
Chemistry and Biodiversity, 2013 , vol. 10, # 9 p. 1559 - 1573
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