4'-叔丁基[1,1'-联苯]-4-醇合成路线 （共 2 条）
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water T=80°C; 48 h;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2006/72015 A2, 2006 ;
Location in patent: Page/Page column 20 ;
反应条件
1: With sodium carbonate; 1-n-butyl-3-methylimidazolium tetrafluoroborate; tetrakis(triphenylphosphine) palladium(0) in water; N,N-dimethyl-formamide T=110°C; Suzuki-Miyaura cross-coupling; 2 h; 2: With trifluoroacetic acid in dichloromethane 1 h; Further stages.;
参考文献
Revell, Jefferson D.; Ganesan
Organic Letters, 2002 , vol. 4, # 18 p. 3071 - 3073
