2-碘-3,5-二甲基苯甲酸合成路线 （共 3 条）
反应条件
1: With sulfuric acid in water T=25°C; 0.2 h; 2: With sodium nitrite in water T=0°C; 1.5 h; 3: With copper; potassium iodide in water T=25°C; 16 h;
参考文献
Moorthy, Jarugu Narasimha; Senapati, Kalyan; Parida, Keshaba Nanda; Jhulki, Samik; Sooraj, Kunnikuruvan; Nair, Nisanth N.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9593 - 9601
反应条件
1.1: sulfuric acid; nitric acid; acetic acid / 0.5 h / 80 °C 2.1: hydrogenchloride; tin / ethanol; water / 1.5 h / 50 - 70 °C 3.1: sulfuric acid / water / 0.2 h / 25 °C 3.2: 1.5 h / 0 °C 3.3: 16 h / 25 °C View Scheme
参考文献
Moorthy, Jarugu Narasimha; Senapati, Kalyan; Parida, Keshaba Nanda; Jhulki, Samik; Sooraj, Kunnikuruvan; Nair, Nisanth N.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9593 - 9601
反应条件
1.1: hydrogenchloride; tin / ethanol; water / 1.5 h / 50 - 70 °C 2.1: sulfuric acid / water / 0.2 h / 25 °C 2.2: 1.5 h / 0 °C 2.3: 16 h / 25 °C View Scheme
参考文献
Moorthy, Jarugu Narasimha; Senapati, Kalyan; Parida, Keshaba Nanda; Jhulki, Samik; Sooraj, Kunnikuruvan; Nair, Nisanth N.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9593 - 9601
