4-甲基-3,4-二氢-2H-1-萘酮合成路线 (共 23 条)
反应条件
SbF5; epoxysulfonyl fluoride in various solvent(s) T=0°C; Friedel-Crafts cyclization; 0.166667 h;
参考文献
Synthesis, , # 1 art. no. F11304SS, p. 39 - 46
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane T=0 - 80°C; 24 h;
参考文献
Organic Letters, , vol. 13, # 24 p. 6488 - 6491
反应条件
tin(IV) chloride; benzene
参考文献
Journal of the American Chemical Society, , vol. 75, p. 347
反应条件
dipotassium peroxodisulfate; silver nitrate in water; acetonitrile T=50°C; Sonogashira Cross-Coupling; 10 h; Inert atmosphere; chemoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 35 p. 14330 - 14333
反应条件
Celite; pyridinium chlorochromate in benzene 14 h; Heating;
参考文献
Synthetic Communications, , vol. 16, # 12 p. 1493 - 1498
反应条件
aluminium trichloride; cyclohexane in dichloromethane 3 h; Ambient temperature; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 5 p. 689 - 693
反应条件
aluminium trichloride 4 h; Heating;
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 3-4 p. 116 - 124
反应条件
aluminium trichloride in dichloromethane 3 h; Ambient temperature; Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 5 p. 689 - 693
反应条件
aluminium trichloride
参考文献
Chemische Berichte, , vol. 94, p. 1717 - 1722
反应条件
1: (i) Mg, (ii) /BRN= 1900390/ 2: AlCl3 View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 31, p. 2143 - 2149,2003 - 2007