4-氨基-N-(2-氯苯基)-苯磺酰胺合成路线 （共 5 条）
反应条件
hydrogen; Raney Ni in ethanol; ethyl acetate P=760.051 Torr; 3 h;
参考文献
MERCK andamp; CO., INC.; MCCAULEY, John, A.; BUTCHER, John, W.; HESS, John, W.; LIVERTON, Nigel, J.; ROMANO, Joseph, J.
Patent: WO2010/33350 A1, 2010 ;
Location in patent: Page/Page column 27 ;
WO 2010/033350 A1
反应条件
hydrogenchloride Heating;
参考文献
Lisitsyn, V. N.; Sazonchik, O. B.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 5.2 p. 780 - 784
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 5 p. 735 - 739
反应条件
1: 82 percent / pyridine / 20 °C 2: 100 percent / Sn; HCl / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Lisitsyn, V. N.; Sazonchik, O. B.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 5.2 p. 780 - 784
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 5 p. 735 - 739
反应条件
1: 82 percent / pyridine / 20 °C 2: 100 percent / Sn; HCl / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
MERCK SHARP and DOHME CORP.; LIVERTON, Nigel; JONES, Philip; LEI, Zhiyu; LIU, Fuqing; LUO, Yunfu; DONG, Jingchao; SOLL, Richard
Patent: WO2013/63100 A1, 2013 ;
反应条件
1: 70 percent / H2O / 1.5 h / 55 - 60 °C 2: 90 percent / 10percent HCl / Heating View Scheme
参考文献
Lisitsyn, V. N.; Sazonchik, O. B.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 5.2 p. 780 - 784
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 5 p. 735 - 739
