(S)-4,5-异亚丙基-2-戊烯溴合成路线 （共 4 条）
反应条件
N-bromosuccinmide; triphenylphosphine in dichloromethane T=0 - 20°C;
参考文献
Ellwood, Adam R.; Mortimer, Anne J. Price; Goodman, Jonathan M.; Porter, Michael J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 43 p. 7530 - 7539
反应条件
1: sodium periodate; sodium hydrogencarbonate / methanol; water / 0 - 20 °C 2: potassium carbonate / water / 0 - 20 °C 3: diisobutylaluminium hydride / dichloromethane / -78 °C 4: N-bromosuccinmide; triphenylphosphine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Ellwood, Adam R.; Mortimer, Anne J. Price; Goodman, Jonathan M.; Porter, Michael J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 43 p. 7530 - 7539
反应条件
1: diisobutylaluminium hydride / dichloromethane / -78 °C 2: N-bromosuccinmide; triphenylphosphine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Ellwood, Adam R.; Mortimer, Anne J. Price; Goodman, Jonathan M.; Porter, Michael J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 43 p. 7530 - 7539
反应条件
1: potassium carbonate / water / 0 - 20 °C 2: diisobutylaluminium hydride / dichloromethane / -78 °C 3: N-bromosuccinmide; triphenylphosphine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Ellwood, Adam R.; Mortimer, Anne J. Price; Goodman, Jonathan M.; Porter, Michael J.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 43 p. 7530 - 7539
