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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1985-32-6
合成路线
（共 54 条）
342-24-5
邻氟二苯甲酮
+
100-58-3
溴化苯基镁
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium bromide With titanium tetraethoxide in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: (2-fluorophenyl)phenylmethanone With tributylphosphine; cobalt(II) chloride in tetrahydrofuran T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Zeng, Jing; Liu, Kun Ming; Duan, Xin Fang
Organic Letters, 2013 , vol. 15, # 20 p. 5342 - 5345
2835-77-0
2-氨基二苯甲酮
+
71-43-2
苯
→
反应条件
486-25-9
9-芴酮
+
1985-32-6
反应条件
toluene-4-sulfonic acid; orthoformic acid triethyl ester; copper(l) chloride; sodium nitrite T=50°C; Gomberg-Bachmann-Hey reaction; 0.75 h; regioselective reaction;
参考文献
Chaturbhuj, Ganesh U.; Akamanchi, Krishnacharya G.
Tetrahedron Letters, 2011 , vol. 52, # 38 p. 4950 - 4953
13047-06-8
2-溴苯基苯甲酮
+
100-59-4
苯基氯化镁
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=-20°C; 0.166667 h; 2: 2-bromobenzophenone With iron (III) acetylacetonate in tetrahydrofuran; ethylene glycol dimethyl ether
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
512787-24-5
+
100-59-4
苯基氯化镁
→
反应条件
1985-32-6
反应条件
1: phenyl-magnesium chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=-20°C; 0.166667 h; 2: 2-benzoylphenyl trifluoromethanesulfonate With iron (III) acetylacetonate in tetrahydrofuran; ethylene glycol dimethyl ether
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
609-67-6
邻碘苯甲酰氯
→
反应条件
1985-32-6
反应条件
MnCl2∙4H2O in tetrahydrofuran T=-30°C; 1 h; Inert atmosphere;
参考文献
Zhang, Fengmin; Shi, Zhuangzhi; Chen, Feng; Yuan, Yu
Applied Organometallic Chemistry, 2010 , vol. 24, # 1 p. 57 - 63
→
反应条件
1985-32-6
反应条件
MnCl2∙4H2O in tetrahydrofuran T=-30°C; 1 h; Inert atmosphere;
参考文献
Zhang, Fengmin; Shi, Zhuangzhi; Chen, Feng; Yuan, Yu
Applied Organometallic Chemistry, 2010 , vol. 24, # 1 p. 57 - 63
2835-77-0
2-氨基二苯甲酮
→
反应条件
1985-32-6
反应条件
1.1: HBr; KNO2 / H2O / 0 - 20 °C 1.2: 68 percent / CuBr; HBr / H2O / 20 - 60 °C 2.1: CuCN*2LiCl / 1,2-dimethoxy-ethane; tetrahydrofuran / 0.17 h / -20 °C 2.2: Fe(acac)3 / 1,2-dimethoxy-ethane; tetrahydrofuran View Scheme
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
13047-06-8
2-溴苯基苯甲酮
+
98-80-6
苯硼酸
→
反应条件
1985-32-6
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; water; toluene 12 h; Inert atmosphereReflux;
参考文献
Zhao, Zujin; He, Bairong; Nie, Han; Chen, Bin; Lu, Ping; Qin, Anjun; Tang, Ben Zhong
Chemical Communications, 2014 , vol. 50, # 9 p. 1131 - 1133
117-99-7
2-羟基二苯甲酮
→
反应条件
1985-32-6
反应条件
1.1: 94 percent / pyridine / 0 - 20 °C 2.1: CuCN*2LiCl / 1,2-dimethoxy-ethane; tetrahydrofuran / 0.17 h / -20 °C 2.2: Fe(acac)3 / 1,2-dimethoxy-ethane; tetrahydrofuran View Scheme
参考文献
Sapountzis, Ioannis; Lin, Wenwei; Kofink, Christiane C.; Despotopoulou, Christina; Knochel, Paul
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1654 - 1657
→
反应条件
1985-32-6
反应条件
MnCl2∙4H2O in tetrahydrofuran T=-30°C; 1 h; Inert atmosphere;
参考文献
Zhang, Fengmin; Shi, Zhuangzhi; Chen, Feng; Yuan, Yu
Applied Organometallic Chemistry, 2010 , vol. 24, # 1 p. 57 - 63
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