7-甲基六氢-1H-氮杂卓-2-酮合成路线 （共 8 条）
反应条件
sodium azide; methanesulfonic acid in ethylene glycol dimethyl ether T=-30 - 20°C; 3 h;
参考文献
Galvez, Nicanor; Moreno-Manas, Marcial; Sebastian, Rosa M.; Vallribera, Adelina
Tetrahedron, 1996 , vol. 52, # 5 p. 1609 - 1616
反应条件
hydrogen; nickel in ethanol T=150°C; P=114000 Torr; 7 h;
参考文献
Nagasaka, Tatsuo; Kato, Hiroki; Hayashi, Hideki; Shioda, Masako; Hikasa, Hiromi; Hamaguchi, Fumiko
Heterocycles, 1990 , vol. 30, # 1 p. 561 - 566
反应条件
indium trifluoromethanesulfonate in acetonitrile Beckmann rearrangement; 3.5 h; Heating;
参考文献
Barman, Dhiren C.; Gohain, Mukut; Prajapati, Dipak; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 1 p. 154 - 156
反应条件
hydrogen; acetic acid; platinum(IV) oxide in ethyl acetate
参考文献
Yamada, Kazutoshi; Tanaka, Seiji; Naruchi, Kiyoshi; Yamamoto, Makoto
Journal of Organic Chemistry, 1982 , vol. 47, # 27 p. 5283 - 5289
反应条件
boron trifluoride diethyl etherate in dichloromethane 16 h; Ambient temperature;
参考文献
Nishiyama, Hisao; Sakuta, Koji; Osaka, Noriyuki; Arai, Hiroyuki; Matsumoto, Makoto; Itoh, Kenji
Tetrahedron, 1988 , vol. 44, # 9 p. 2413 - 2426
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate 58 h; Ambient temperature;
参考文献
Yoshifuji, Shigeyuki; Arakawa, Yukimi; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 1 p. 357 - 363
反应条件
sulfuric acid T=120°C; Title compound not separated from byproducts;
参考文献
Hermecz, Istvan; Vasvari-Debreczy, Lelle; Horvath, Agnes; Balogh, Maria; Koekoesi, Jozsef; et al.
Journal of Medicinal Chemistry, 1987 , vol. 30, # 9 p. 1543 - 1549
参考文献
Mueller; Krauss
Monatshefte fuer Chemie, 1932 , vol. 61, p. 221
