1,4-双(2-苯乙基)苯合成路线 （共 15 条）
反应条件
1: With tris-(dibenzylideneacetone)dipalladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=20°C; 0.25 h; Inert atmosphere;
2: With formic acid in 1,4-dioxane
T=80°C; Inert atmosphere; chemoselective reaction;
参考文献
Shen, Ruwei; Chen, Tieqiao; Zhao, Yalei; Qiu, Renhua; Zhou, Yongbo; Yin, Shuangfeng; Wang, Xiangbo; Goto, Midori; Han, Li-Biao
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 17037 - 17044
参考文献
Lai,L.-F.; Tidwell,T.T.
Journal of the American Chemical Society, 1977 , vol. 99, # 5 p. 1465 - 1470
反应条件
1: Py / pentane; diethyl ether
2: toluene / 100 °C
View Scheme
参考文献
Lai,L.-F.; Tidwell,T.T.
Journal of the American Chemical Society, 1977 , vol. 99, # 5 p. 1465 - 1470
反应条件
1: SnCl2, aq. HCl / tetrahydrofuran
2: H2 / Pd-C / tetrahydrofuran
View Scheme
参考文献
Misumi,S.
Bulletin of the Chemical Society of Japan, 1961 , vol. 34, p. 1827 - 1832
反应条件
1: (i) NaNH2, liq. NH3, Et2O, (ii) /BRN= 773967/
2: SnCl2, aq. HCl / tetrahydrofuran
3: H2 / Pd-C / tetrahydrofuran
View Scheme
参考文献
Misumi,S.
Bulletin of the Chemical Society of Japan, 1961 , vol. 34, p. 1827 - 1832
反应条件
1: NaOMe / methanol
2: H2, AcOH / PtO2
View Scheme
参考文献
Agranat,I.; Avnir,D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 1155 - 1161
反应条件
1: NaOMe / methanol
2: H2, AcOH / PtO2
View Scheme
参考文献
Agranat,I.; Avnir,D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 1155 - 1161
反应条件
hydrogen; acetic acid; platinum(IV) oxide
参考文献
Agranat,I.; Avnir,D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 1155 - 1161
反应条件
copper in quinoline
Heating;
参考文献
Agranat,I.; Avnir,D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 1155 - 1161
反应条件
1: AlCl3
2: N2H4+H2O
View Scheme
参考文献
Schmitt et al.
Bulletin de la Societe Chimique de France, 1955 , p. 1055,1058
