Fmoc-L-炔丙基甘氨酸合成路线 （共 6 条）
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water T=20°C;
参考文献
Byrne, Cillian; McEwan, Paul A.; Emsley, Jonas; Fischer, Peter M.; Chan, Weng C.
Chemical Communications, 2011 , vol. 47, # 9 p. 2589 - 2591
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 15 h;
参考文献
Itoh, Hiroaki; Matsuoka, Shigeru; Kreir, Mohamed; Inoue, Masayuki
Journal of the American Chemical Society, 2012 , vol. 134, # 34 p. 14011 - 14018
反应条件
potassium carbonate in 1,4-dioxane; water T=0°C; 0.5 h; Inert atmosphere;
参考文献
Sminia, Tjerk Jacco; Pedersen, Daniel Sejer
Synlett, 2012 , vol. 23, # 18 p. 2643 - 2646,4
Title/Abstract Full Text Show Details
Sminia, Tjerk Jacco; Pedersen, Daniel Sejer
Synlett, 2012 , vol. 23, # 18 p. 2643 - 2646
反应条件
1: sodium hydrogencarbonate / water; 1,4-dioxane / 4 h / 20 °C 2: trifluoroacetic acid / dichloromethane / 15 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 34 p. 14011 - 14018
反应条件
1: citric acid / water; tetrahydrofuran / 21 h / 20 °C 2: sodium hydrogencarbonate / water; 1,4-dioxane / 4 h / 20 °C 3: trifluoroacetic acid / dichloromethane / 15 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 34 p. 14011 - 14018
反应条件
[Rh(COD)(1,4-bis(diphenylphosphino)butane)]BF4; hydrogen in methanol-d4 P=1500.15 Torr; 0.00277778 h;
参考文献
Koerner, Marco; Sauer, Grit; Heil, Andreas; Nasu, Daichi; Empting, Martin; Tietze, Daniel; Voigt, Stephan; Weidler, Heiko; Gutmann, Torsten; Avrutina, Olga; Kolmar, Harald; Ratajczyk, Tomasz; Buntkowsky, Gerd
Chemical Communications, 2013 , vol. 49, # 71 p. 7840 - 7841
