1,2-o-异亚丙基-3-苄氧基-5,6-二脱氧-呋喃葡萄糖合成路线 （共 19 条）
反应条件
(3a,9R,3'''a,4'"b,9'"R)-9,9'-[1,4-phthalazinediylbis(oxy)]bis[6'-(methyloxy)-10,11-dihydrocinchonan]; N-methyl-2-indolinone; polysulfone microencapsulated OsO4 in water; acetone; acetonitrile T=20°C; 0.416667 h;
参考文献
Malla Reddy; Srinivasulu; Venkat Reddy; Narasimhulu; Venkateswarlu
Tetrahedron Letters, 2006 , vol. 47, # 30 p. 5285 - 5288
反应条件
AD-mix-α in water; tert-butyl alcohol T=0°C; Sharpless asymmetric dihydroxylation; 96 h; Title compound not separated from byproducts;
参考文献
Mereyala, Hari Babu; Goud, P. Mallikarjun; Gadikota, Rajendrakumar Reddy; Maddala, Rama Krishna; Reddy, K. Ramasubba
Journal of Carbohydrate Chemistry, 2000 , vol. 19, # 9 p. 1201 - 1210
反应条件
sodium iodide in butanone
24 h; Heating;
参考文献
Sherk, Alfred E.; Fraser-Reid, Bert
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 932 - 935
反应条件
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane
0.5 h;
2: (3aR,5S,6S,6aR)-6-(benzyloxy)-tetrahydro-2,2-dimethylfuro[2,3-d][1,3]dioxol-5-carbaldehyde in tetrahydrofuran; hexane
T=0°C; 3 h; Inert atmosphere;
参考文献
Hsu, Ching-Yun; Lee, I-Chi; Lico, Larry S.; Uang, Biing-Jiun; Hung, Shang-Cheng
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 3 p. 421 - 425
反应条件
acetone; sodium iodide
T=125°C;
参考文献
English; Levy
Journal of the American Chemical Society, 1956 , vol. 78, p. 2846
反应条件
sodium hydride in N,N-dimethyl-formamide
1.5 h; Ambient temperature;
参考文献
Krohn, Karsten; Ekkundi, Vadiraj S.; Doering, Detlev; Jones, Peter
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 2 p. 153 - 170
反应条件
1H-imidazole; iodine; chloro-diphenylphosphine; zinc
1) toluene, reflux, 30 min, 2) reflux, 30 min; Yield given. Multistep reaction;
参考文献
Liu, Zhengchun; Classon, Bjoern; Samuelsson, Bertil
Journal of Organic Chemistry, 1990 , vol. 55, # 14 p. 4273 - 4275
反应条件
1: 100 percent / acetone / Ambient temperature
2: 94 percent / NaBH4 / methanol / Ambient temperature
View Scheme
参考文献
Calvo-Flores, Francisco G.; Garcia-Mendoza, Pilar; Hernandez-Mateo, Fernando; Isac-Garcia, Joaquin; Santoyo-Gonzalez, Francisco
Journal of Organic Chemistry, 1997 , vol. 62, # 12 p. 3944 - 3961
反应条件
1: 83 percent / NaIO4, RuCl3*3H2O / acetonitrile; CCl4; H2O / Ambient temperature
2: 100 percent / acetone / Ambient temperature
3: 94 percent / NaBH4 / methanol / Ambient temperature
View Scheme
参考文献
Calvo-Flores, Francisco G.; Garcia-Mendoza, Pilar; Hernandez-Mateo, Fernando; Isac-Garcia, Joaquin; Santoyo-Gonzalez, Francisco
Journal of Organic Chemistry, 1997 , vol. 62, # 12 p. 3944 - 3961
反应条件
diethylamino-sulfur trifluoride in dichloromethane
a) -10 deg C, 0.5 h, b) RT, 1 h;
参考文献
Mori, Yoko; Morishima, Naohiko
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 1 p. 236 - 241
