1-硫代-b-D-葡萄糖四乙酸酯合成路线 (共 55 条)
反应条件
sodium hydrogensulfite in water T=0°C; 2 h;
参考文献
Yu, Zhiqiang; Cui, Mengmeng; Yan, Junjie; You, Yezi
Science China Chemistry, 2010 , vol. 53, # 8 p. 1663 - 1668
反应条件
carbon disulfide; Na2S*9H2O in N,N-dimethyl-formamide T=20°C; 0.0833333 h; SolventTime; stereoselective reaction;
参考文献
Jana, Manas; Misra, Anup Kumar
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2680 - 2686
反应条件
Lawesson's reagent in 1,4-dioxane T=110°C; 72 h;
参考文献
Bernardes, Goncalo J. L.; Gamblin, David P.; Davis, Benjamin G.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 24 p. 4007 - 4011
反应条件
sodium thiomethoxide in methanol; dichloromethane T=0°C; 0.0833333 h;
参考文献
MacDougall, James M.; Zhang, Xiao-Dong; Polgar, Willma E.; Khroyan, Taline V.; Toll, Lawrence; Cashman, John R.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 23 p. 5809 - 5815
反应条件
sodium dithionite in dichloromethane; water T=50°C; 2 h;
参考文献
Fan, Wei; Yan, Chengyi; Qian, Shan; Yao, Nian; Tang, Lei; Wu, Yong
Letters in Drug Design and Discovery, 2010 , vol. 7, # 4 p. 281 - 289
反应条件
4-methyl-morpholine in dichloromethane T=40 - 42°C; 12 h;
参考文献
Ljevakovic, Durdica; Tomic, Srdanka; Tomasic, Jelka; Horvat, Jaroslav
Croatica Chemica Acta, 1996 , vol. 69, # 4 p. 1329 - 1337
反应条件
4-methyl-morpholine in dichloromethane T=40 - 42°C; 12 h;
参考文献
Ljevakovic, Durdica; Tomic, Srdanka; Tomasic, Jelka; Horvat, Jaroslav
Croatica Chemica Acta, 1996 , vol. 69, # 4 p. 1329 - 1337
反应条件
4-methyl-morpholine in dichloromethane T=40 - 42°C; 12 h;
参考文献
Ljevakovic, Durdica; Tomic, Srdanka; Tomasic, Jelka; Horvat, Jaroslav
Croatica Chemica Acta, 1996 , vol. 69, # 4 p. 1329 - 1337
反应条件
boron trifluoride diethyl etherate; thiourea
参考文献
Journal of Medicinal Chemistry, , vol. 52, # 20 p. 6421 - 6432
反应条件
4-methyl-morpholine in dichloromethane T=40 - 42°C; 12 h;
参考文献
Ljevakovic, Durdica; Tomic, Srdanka; Tomasic, Jelka; Horvat, Jaroslav
Croatica Chemica Acta, 1996 , vol. 69, # 4 p. 1329 - 1337