3,5-二叔丁基-4-羟基苯甲腈合成路线 （共 19 条）
反应条件
ammonium hydroxide; oxygen in propan-1-ol T=88°C; 1 h; var. temp., time, aldehyde conc.; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 8.2 p. 1540 - 1548
Zhurnal Organicheskoi Khimii, , vol. 25, # 8 p. 1706 - 1715
反应条件
potassium hydroxide in glycerol T=200°C;
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
hydrogenchloride Erwaermen des Reaktionsprodukts mit NaHCO3 in wss. Aethanol;
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
sulfuric acid Heating;
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
1: KOH / glycerol / 200 °C 2: diethyl ether View Scheme
参考文献
Mueller,E. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 645, p. 36 - 52
反应条件
sulfuric acid Heating;
参考文献
Teubner,H.-J. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 757 - 770
反应条件
lithium aluminium tetrahydride
参考文献
Mueller et al.
Chemische Berichte, 1959 , vol. 92, p. 2278,2290
反应条件
hydrogenchloride; aluminum tri-bromide; lt;3,5-di(tert-butyl)gt;-4-hydroxybenzoic acid nitrile in diethyl ether
a) 20 deg C, 12 h, b) 145 deg C, 12 h;
参考文献
Kelarev, V. I.; Koshelev, V. N.; Belov, N. V.; Malova, O. V.; Karakhanov, R. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1994 , vol. 30, # 2 p. 218 - 221
Khimiya Geterotsiklicheskikh Soedinenii, 1994 , # 2 p. 240 - 243
参考文献
Mueller et al.
Chemische Berichte, 1959 , vol. 92, p. 2278,2290
