3-氯-2,3-双(4-甲氧基苯基)丙烯醛合成路线 (共 3 条)
反应条件
1: With trichlorophosphate T=20°C; 1 h; 2: With sodium acetate cooling; Further stages.;
参考文献
European Journal of Medicinal Chemistry, , vol. 43, # 6 p. 1152 - 1159
反应条件
1: With trichlorophosphate in dichloromethane Substitution; 5 h; Heating; 2: With water in tetrahydrofuran T=25°C; Hydrolysis; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 55, # 51 p. 14515 - 14522
反应条件
1.1: 91 percent / dimethylformamide / 18 h / Heating 2.1: POCl3 / CH2Cl2 / 5 h / Heating 2.2: H2O / tetrahydrofuran / 25 °C View Scheme
参考文献
Tetrahedron, , vol. 55, # 51 p. 14515 - 14522