1,2-二(4,4-二甲基-2-噁唑并英-2-基)乙烷合成路线 (共 4 条)
反应条件
KNH2 in diethyl ether; ammonia 1 h; Irradiation;
参考文献
Wong, Jim-Wah; Natalie Jr., Kenneth J.; Nwokogu, Godson C.; Pisipati, Jyothi S.; Flaherty, Patrick T.; Greenwood, Thomas D.; Wolfe, James F.
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6152 - 6159
反应条件
T=170°C; 0.416667 h; Microwave irradiationNeat (no solvent)open vessel;
参考文献
Sharma, Rishi; Vadivel, Subramanian K.; Duclos Jr., Richard I.; Makriyannis, Alexandros
Tetrahedron Letters, 2009 , vol. 50, # 42 p. 5780 - 5782
反应条件
KNH2 1) liq. NH3, -33 deg C, 15 min; 2) irradiation, 5 min, liq. NH3, -33 deg C; further reagents and conditions; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wong, Jim-Wah; Natalie Jr., Kenneth J.; Nwokogu, Godson C.; Pisipati, Jyothi S.; Flaherty, Patrick T.; Greenwood, Thomas D.; Wolfe, James F.
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6152 - 6159
反应条件
KNH2 1) liq. NH3, -33 deg C, 15 min; 2) irradiation, 5 min, liq. NH3, -33 deg C; further conditions; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wong, Jim-Wah; Natalie Jr., Kenneth J.; Nwokogu, Godson C.; Pisipati, Jyothi S.; Flaherty, Patrick T.; Greenwood, Thomas D.; Wolfe, James F.
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6152 - 6159