9,9-二辛基-2,7-二溴代芴合成路线 （共 30 条）
反应条件
sodium hydroxide; n-butyllithium 2.) ether, reflux; Yield givenMultistep reaction;
参考文献
Intemann, Jeremy J.; Mike, Jared F.; Cai, Min; Barnes, Charles A.; Xiao, Teng; Roggers, Robert A.; Shinar, Joseph; Shinar, Ruth; Jeffries-El, Malika
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 4 p. 916 - 923
反应条件
potassium carbonate; Pd(0)(PPh3)4 in toluene
参考文献
Tsuda, Yoshihiro; Morishita, Yoshii; Nomura, Satoyuki; Tai, Seiji; Hoshi, Yousuke; Funyuu, Shigeaki; Motamedi, Farshad J.; Wang, Li-Sheng
Patent: US2006/247474 A1, 2006 ;
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78 - 20°C; 3: With hydrogenchloride in tetrahydrofuran; hexane; water
参考文献
Elmalem, Einat; Kiriy, Anton; Huck, Wilhelm T. S.
Macromolecules, 2011 , vol. 44, # 22 p. 9057 - 9061
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=0°C; 2: With methanol in tetrahydrofuran; hexane T=0°C;
参考文献
Nagaki, Aiichiro; Takabayashi, Naofumi; Tomida, Yutaka; Yoshida, Jun-Ichi
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. A16
反应条件
1: in tetrahydrofuran; hexane T=0°C; 0.166667 h; 2: With methanol in tetrahydrofuran; hexane T=-78°C; 0.166667 h;
参考文献
Nagaki, Aiichiro; Takabayashi, Naofumi; Tomida, Yutaka; Yoshida, Jun-ichi
Organic Letters, 2008 , vol. 10, # 18 p. 3937 - 3940
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=0°C; 1.58333E-05 h; flow conditions; 2: With methanol in tetrahydrofuran; hexane T=0°C; flow conditions;
参考文献
Nagaki, Aiichiro; Takabayashi, Naofumi; Tomida, Yutaka; Yoshida, Jun-Ichi
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. A16
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.166667 h; 2: With methanol in tetrahydrofuran; hexane 0.166667 h;
参考文献
Nagaki, Aiichiro; Takabayashi, Naofumi; Tomida, Yutaka; Yoshida, Jun-Ichi
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. A16
反应条件
1: 2,7-dibromo-9,9-di-n-octylfluorene With n-butyllithium in tetrahydrofuran; hexane T=-78 - 0°C; 0.616667 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexane T=-78 - 20°C; 30 h;
参考文献
Pasini, Mariacecilia; Destri, Silvia; Porzio, William; Botta, Chiara; Giovanella, Umberto
Journal of Materials Chemistry, 2003 , vol. 13, # 4 p. 807 - 813
反应条件
1: 2,7-dibromo-9,9-di-n-octylfluorene With n-butyllithium T=-78°C; 2: iPrB(pinacolate)
参考文献
Yang, Renqiang; Tian, Renyu; Yan, Jingai; Zhang, Yong; Yang, Jian; Hou, Qiong; Yang, Wei; Zhang, Chi; Cao, Yong
Macromolecules, 2005 , vol. 38, # 2 p. 244 - 253
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in dimethyl sulfoxide
参考文献
Zhang, Ting; Deng, Lijun; Wang, Renjie; Zhou, Wei; Li, Jiuyan
Dyes and Pigments, 2012 , vol. 94, # 3 p. 380 - 385
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Zhang, Ting; Wang, Renjie; Ren, Huicai; Chen, Zhiguang; Li, Jiuyan
Polymer, 2012 , vol. 53, # 7 p. 1529 - 1534
