(1-(4-甲氧基苄基)-1H-1,2,4-噻唑-5-基)甲胺合成路线 (共 5 条)
反应条件
hydrazine hydrate in methanol Ambient temperature;
参考文献
Urban, Frank J.; Breitenbach, Ralph
Synthetic Communications, 1999 , vol. 29, # 4 p. 645 - 653
反应条件
1: 56 percent / 96 h / 130 °C 2: 91 percent / diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature 3: 97 percent / N2H4*H2O / methanol / Ambient temperature View Scheme
参考文献
Urban, Frank J.; Breitenbach, Ralph
Synthetic Communications, 1999 , vol. 29, # 4 p. 645 - 653
反应条件
1: 69 percent / NaOH / dimethylformamide / 4 h / Ambient temperature 2: 56 percent / 96 h / 130 °C 3: 91 percent / diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature 4: 97 percent / N2H4*H2O / methanol / Ambient temperature View Scheme
参考文献
Urban, Frank J.; Breitenbach, Ralph
Synthetic Communications, 1999 , vol. 29, # 4 p. 645 - 653
反应条件
1: 91 percent / diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature 2: 97 percent / N2H4*H2O / methanol / Ambient temperature View Scheme
参考文献
Urban, Frank J.; Breitenbach, Ralph
Synthetic Communications, 1999 , vol. 29, # 4 p. 645 - 653
反应条件
sodium tetrahydroborate in tetrahydrofuran 0.0833333 h; Ambient temperaturereduction of saturated and unsaturated alkyl halides, halo esters, chloroacetanilides with NaBH4; Product distribution;
参考文献
Narasimhan; Swarnalakshmi; Balakumar; Velmathi
Synthetic Communications, 1999 , vol. 29, # 4 p. 685 - 689