2,3,3-三甲基-丁酸甲酯合成路线 (共 13 条)
反应条件
1: 71 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
2: 64 percent / Dess-Martin periodinane / CH2Cl2 / 1 h / 20 °C
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参考文献
Arjona, Odon; Perez-Ossorio, Rafael; Perez-Rubalcaba, Alfredo; Quiroga, Maria L.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 597 - 603
反应条件
1: NaOH / bis-(2-hydroxy-ethyl) ether
2: PhCOCl
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参考文献
Saunders,W.H.; Carges,G.L.
Journal of the American Chemical Society, 1960 , vol. 82, p. 3582 - 3585
反应条件
1: NaOH / bis-(2-hydroxy-ethyl) ether
2: PhCOCl
3: (i) Mg, Et2O, CdCl2, (ii) /BRN= 1747009/
View Scheme
参考文献
Saunders,W.H.; Carges,G.L.
Journal of the American Chemical Society, 1960 , vol. 82, p. 3582 - 3585