2-(三氟甲基)苯基三氟甲烷磺酸酯合成路线 （共 3 条）
反应条件
pyridine T=0 - 20°C; 48 h;
参考文献
Dyke, Alan M.; Gill, Duncan M.; Harvey, Jeremy N.; Hester, Alison J.; Lloyd-Jones, Guy C.; Munoz, M. Paz; Shepperson, Ian R.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 27 p. 5067 - 5070
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide in N,N-dimethyl-formamide T=70°C; 4 h;
参考文献
Qing, Feng-Ling; Fan, Junfa; Sun, Hong-Bin; Yue, Xiang-Jun
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 3053 - 3057
反应条件
1: 84 percent / Et3N / CH2Cl2 / 1.) -78 deg C, 1.5 h, 2.) -78 deg C to r.t., overnight 2: 84 percent / CuI, HMPA / dimethylformamide / 4 h / 70 °C View Scheme
参考文献
Qing, Feng-Ling; Fan, Junfa; Sun, Hong-Bin; Yue, Xiang-Jun
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 3053 - 3057
