3-(三氟甲基)苯基三氟甲烷磺酸酯合成路线 （共 8 条）
反应条件
pyridine T=0 - 20°C; 48 h;
参考文献
Gill, Duncan; Hester, Alison J.; Lloyd-Jones, Guy C.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2547 - 2548
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide in N,N-dimethyl-formamide T=70°C;
参考文献
Qing, Feng-Ling; Fan, Junfa; Sun, Hong-Bin; Yue, Xiang-Jun
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 3053 - 3057
反应条件
pyridine T=90°C; 1 h;
参考文献
Yoneda, Norihiko; Fukuhara, Tsuyoshi; Mizokami, Takao; Suzuki, Akira
Chemistry Letters, 1991 , # 3 p. 459 - 460
参考文献
Yoneda, Norihiko; Fukuhara, Tsuyoshi; Mizokami, Takao; Suzuki, Akira
Chemistry Letters, 1991 , # 3 p. 459 - 460
反应条件
1: 78 percent / Et3N / CH2Cl2 2: 64 percent / CuI, HMPA / dimethylformamide / 70 °C View Scheme
参考文献
Qing, Feng-Ling; Fan, Junfa; Sun, Hong-Bin; Yue, Xiang-Jun
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 3053 - 3057
反应条件
1: 1,1'-bis-(diphenylphosphino)ferrocene; [Ni0(1,5-cyclooctadiene)2]; N,N-dicyclohexylmethylamine / 1,4-dioxane / 20 h / 100 °C / Inert atmosphere 2: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C / Inert atmosphere View Scheme
参考文献
Gogsig, Thomas M.; Kleimark, Jonatan; Nilsson Lill, Sten O.; Korsager, Signe; Lindhardt, Anders T.; Norrby, Per-Ola; Skrydstrup, Troels
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 443 - 452
反应条件
1: With Zn[N(SiMe3)2]2; tri-tert-butyl phosphine; tetrabutylammomium bromide; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=50°C; 6 h; 2: With hydrogenchloride in tetrahydrofuran; diethyl ether
参考文献
Lee, Dae-Yon; Hartwig, John F.
Organic Letters, 2005 , vol. 7, # 6 p. 1169 - 1172
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene T=100°C; 1.5 h;
参考文献
Journal of Organic Chemistry, , vol. 74, # 13 p. 4720 - 4726
