1: (i) Mg, Et2O, benzene, (ii) aq. HCl, (iii) I2 2: dimethylformamide 3: aq. KOH / ethane-1,2-diol 4: H2 / Pd-C / dimethylformamide View Scheme

1: (i) Mg, Et2O, benzene, (ii) aq. HCl, (iii) I2 2: dimethylformamide 3: aq. KOH / ethane-1,2-diol 4: H2 / Pd-C / dimethylformamide View Scheme

暂无反应条件数据

1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 15 h / 90 °C / |Inert atmosphere 2: palladium 10 on activated carbon; hydrogen / methanol / 24 h / 20 °C 3: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C View Scheme

1: 4-(N,N-dimethlyamino)pyridine / tert-butyl alcohol / 12 h / 20 °C 2: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 15 h / 90 °C / |Inert atmosphere 3: palladium 10 on activated carbon; hydrogen / methanol / 24 h / 20 °C 4: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C View Scheme

1: AlCl3 2: AlCl3 3: NaOBr View Scheme

1: AlCl3 2: NaOBr View Scheme

1: AlCl3 2: AlCl3 3: NaOBr View Scheme

1: BF3 2: LiAlH4 3: pyridinium chlorochromate View Scheme