199620-14-9合成路线 (共 107 条)
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.2.1.5.2, page 66 - 70
反应条件
in diethylene glycol thermal reaction;
反应条件
in decane; cyclohexane Kinetics; at 122.5 .+-. °C.;
参考文献
Chemische Berichte, , vol. 99, p. 3582 - 3592
反应条件
High Pressure; thermal reaction;
参考文献
Matthews, C. N.
Patent: US3117983 , 1964 ;
反应条件
in decane; cyclohexane Kinetics; at 122.5 .+-. 0.3 °C.;
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.2.1.5.2, page 66 - 70
反应条件
in tetrahydrofuran Irradiation (UV/VIS); (Ar); drowise addn. of (Ph2Sb)2GeMe2 to irradiated soln. of Cr(CO)6;
参考文献
Breunig, H. J.; Knobloch, T. P.
Journal of Inorganic and Nuclear Chemistry, 1980 , vol. 42, p. 505 - 508
反应条件
in tetrahydrofuran Irradiation (UV/VIS); (Ar); drowise addn. of (Ph2Sb)2GeMe2 to irradiated soln. of Cr(CO)6;
参考文献
Breunig, H. J.; Knobloch, T. P.
Journal of Inorganic and Nuclear Chemistry, 1980 , vol. 42, p. 505 - 508
反应条件
benzene in decalin byproducts: CO; refluxing for 5.5 h (catalyst: butyl acetate); freezing out at -18°C or quick chromy. of the decaline soln. on a SiO2 column;
参考文献
Hudecek, Milan; Gajda, Vladimir; Toma, Stefan
Journal of Organometallic Chemistry, 1991 , vol. 413, # 1-3 p. 155 - 160
反应条件
in tetrahydrofuran; anhydrous butyl ether T=160°C;
参考文献
Ricci, Paolo; Kraemer, Katrina; Cambeiro, Xacobe C.; Larrosa, Igor
Journal of the American Chemical Society, 2013 , vol. 135, # 36 p. 13258 - 13261
反应条件
in tetrahydrofuran; anhydrous butyl ether (under N2); ratio aryl-compd.:Cr(CO)6 1:1, reflux for 100 h in Bu2O-THF; removal of the solvents, sublimation of the residue;
参考文献
Beckett, Michael A.; Gilmore, Robert J.; Idrees, Khalid
Journal of Organometallic Chemistry, 1993 , vol. 455, # 1-2 p. 47 - 49