199620-14-9合成路线 （共 107 条）
反应条件
in tetrahydrofuran; anhydrous butyl ether refluxing for 1 wk; evapn. of solvents under vac., removing unreacted (Cr(CO)6) by sublimation, recrystn. from CH2Cl2 under N2;
参考文献
Chudek, John A.; Hunter, Geoffrey; MacKay, Regine Louise; Kremminger, Peter; Schloegl, Karl; Weissensteiner, Walter
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , p. 2001 - 2006
参考文献
Gmelin Handbook: Cr: Org.Verb., 1.1.2.1.5.2, page 66 - 70
反应条件
in neat (no solvent) passing gaseous C5H6 in a stream of N2 over Cr(CO)6 at 100-120°C; then heating to 280-300°C;;
反应条件
in solid matrix Irradiation (UV/VIS); irradiation of matrix doped with Cr(CO)6 and (13)CO2;
参考文献
Almond, Matthew J.; Downs, Anthony J.; Perutz, Robin N.
Inorganic Chemistry, 1985 , vol. 24, p. 275 - 281
反应条件
catalyst: dimethyl succinate in decalin byproducts: CO; refluxing for 2.3 h (catalyst: dimethyl succinate); freezing out at -18°C or quick chromy. of the decaline soln. on a SiO2 column;
参考文献
Journal of Organometallic Chemistry, , vol. 413, # 1-3 p. 155 - 160
反应条件
acetic acid in decalin refluxing for 2.75 h;
参考文献
Journal of Organometallic Chemistry, , vol. 413, # 1-3 p. 161 - 164
反应条件
formic acid in decalin refluxing for 6-7 h;
参考文献
Journal of Organometallic Chemistry, , vol. 413, # 1-3 p. 161 - 164
反应条件
propionic acid in decalin refluxing for 6-7 h;
参考文献
Journal of Organometallic Chemistry, , vol. 413, # 1-3 p. 161 - 164
反应条件
in tetrahydrofuran; anhydrous butyl ether (under N2); ratio aryl-compd.:Cr(CO)6 1:1, reflux for 48 h in Bu2O-THF; removal of the solvents, sublimation of the residue;
参考文献
Journal of Organometallic Chemistry, , vol. 455, # 1-2 p. 47 - 49
反应条件
in toluene; benzene boiling;;
参考文献
Inorganic Chemistry, , vol. 3, p. 257 - 259
