2-(甲基巯基)-2-噻唑啉合成路线 （共 16 条）
参考文献
Gabriel
Chemische Berichte, 1889 , vol. 22, p. 1138
Chemische Berichte, 1891 , vol. 24, p. 1110
反应条件
potassium hydrogencarbonate in methanol 23 h; Heating;
参考文献
Isoda, Takeshi; Ushirogochi, Hideki; Satoh, Koichi; Takasaki, Tsuyoshi; Yamamura, Itsuki; Sato, Chisato; Mihira, Ado; Abe, Takao; Tamai, Satoshi; Yamamoto, Shigeki; Kumagai, Toshio; Nagao, Yoshimitsu
Journal of Antibiotics, 2006 , vol. 59, # 4 p. 241 - 247
反应条件
1: With methanesulfonic acid in butan-1-ol
T=125°C; 16 h; Heating / reflux;
2: With hydrogenchloride in diethyl ether; water
3: With sodium hydroxide in diethyl ether; water
Product distribution / selectivity;
参考文献
SYNGENTA PARTICIPATIONS AG; SYNGENTA LIMITED
Patent: WO2007/20377 A2, 2007 ;
Location in patent: Page/Page column 149 ;
反应条件
in ethanol
48 h; Heating;
参考文献
Bigg; Purvis
Journal of Heterocyclic Chemistry, 1976 , vol. 13, # 5 p. 977 - 979
反应条件
in ethanol
48 h; Heating;
参考文献
Bigg; Purvis
Journal of Heterocyclic Chemistry, 1976 , vol. 13, # 5 p. 977 - 979
反应条件
acetic acid
T=100°C; 10 h;
参考文献
Chowdhury; Shibata; Morita; Kaya; Hiratani
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 5 p. 1173 - 1177
