1-(三甲基硅氧基)环戊烯合成路线 （共 155 条）
反应条件
1: 84 percent / TiCl4
2: 95 percent / H+
4: 100 percent / H3O+
View Scheme
参考文献
Cherkauskas, John P.; Cohen, Theodore
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 6 - 8
反应条件
aluminum oxide; zinc(II) chloride in tetrahydrofuran
T=0 - 5°C; 1.5 h;
参考文献
Ranu, Brindaban C.; Saha, Manika; Bhar, Sanjay
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 15 p. 2197 - 2200
反应条件
in 1,2-dichloro-ethane
T=25°C; 2.5 h;
参考文献
Hofmann, Karin; Simchen, Gerhard
Liebigs Annalen der Chemie, 1984 , # 1 p. 39 - 47
反应条件
trimethylsilyl iodide in dichloromethane
T=-78°C; 0.833333 h;
参考文献
Sakurai, Hideki; Sasaki, Koshi; Hosomi, Akira
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 10 p. 3195 - 3196
反应条件
tin(IV) chloride in dichloromethane
1.) -78 deg C, 1.5 h, 2.) -78 deg C to r.t.;
参考文献
Braga, Antonio L.; Dornelles, Luciano; Silveira, Claudio C.; Wessjohann, Ludger A.
Synthesis, 1999 , # 4 p. 562 - 564
反应条件
zinc(II) chloride in ethyl acetate
Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Makin, S. M.; Kruglikova, R. I.; Tagirov, T. K.; Kharitonova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1075 - 1078
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1182 - 1185
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Heating;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
zinc(II) chloride in dichloromethane
1 h; Ambient temperature;
参考文献
Reetz, M.T.; Huettenhain, S.H.
Synthesis, 1980 , # 11 p. 941 - 942
反应条件
zinc(II) chloride in dichloromethane
1 h; Ambient temperature;
参考文献
Reetz, M.T.; Huettenhain, S.H.
Synthesis, 1980 , # 11 p. 941 - 942
反应条件
hydrogenchloride; potassium tert-butylate
1) hexane, -70 deg C; 2) 0 deg C, 1.5 h; Yield given. Multistep reaction;
参考文献
Blanco, Luis; Rousseau, Gerard
Bulletin de la Societe Chimique de France, 1985 , # 3 p. 455 - 462
