1-(三甲基硅氧基)环戊烯合成路线 （共 155 条）
反应条件
triethylamine in dichloromethane
1.) -78 deg C; 2.) rt, 1 h;
参考文献
Bannai, Kiyoshi; Toru, Takeshi; Oba, Takeo; Tanaka, Toshio; Noriaki, Okamura; et al.
Tetrahedron, 1983 , vol. 39, # 22 p. 3807 - 3820
反应条件
α-cyclohexylcyclohexanemethanamine; trimethylsilyl iodide in acetonitrile
4 h; Ambient temperature;
参考文献
Hosomi, Akira; Iijima, Susumu; Sakurai, Hideki
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 547 - 550
反应条件
3-chloro-benzenecarboperoxoic acid; sodium iodide in tetrahydrofuran; dichloromethane
T=0°C; 0.166667 h;
参考文献
Sha, Chin-Kang; Young, Jenn-Jong; Jean, Tsong-shin
Journal of Organic Chemistry, 1987 , vol. 52, # 17 p. 3919 - 3920
反应条件
2: 1percent hydrochloric acid / methanol
3: tetra-n-butylammonium fluoride / dimethylsulfoxide / further reagents and solvents
View Scheme
参考文献
Paquette, Leo A.; Valpey, Richard S.; Annis, Gary D.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1317 - 1319
反应条件
samarium (III) iodide in tetrahydrofuran
6 h; Ambient temperature;
参考文献
Bao, Weiliang; Zhang, Yongmin; Ying, Taokai
Synthetic Communications, 1996 , vol. 26, # 3 p. 503 - 507
反应条件
in diethyl ether
T=-20°C; 2 h;
参考文献
Effenberger, Franz; Ziegler, Thomas; Schoenwaelder, Karl-Heinz; Kesmarszky, Thomas; Bauer, Bernd
Chemische Berichte, 1986 , vol. 119, # 11 p. 3394 - 3404
反应条件
bismuth(III) chloride; sodium iodide in diethyl ether; dichloromethane
0.333333 h; Ambient temperature;
参考文献
Le Roux, Christophe; Mandrou, Stephanie; Dubac, Jacques
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3885 - 3887
反应条件
antimony trichloride in dichloromethane
T=0°C; 1 h;
参考文献
Tirpak, Robin E.; Rathke, Michael W.
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5099 - 5102
反应条件
4-pyrrolidin-1-ylpyridine
参考文献
Rasmussen,J.K.
Synthesis, 1977 , p. 91 - 110
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; methyllithium; dimethyl zinc in tetrahydrofuran
T=-60°C; 10 h;
参考文献
Morita, Yasushi; Suzuki, Masaaki; Noyori, Ryoji
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1785 - 1787
