1-(三甲基硅氧基)环戊烯合成路线 （共 155 条）
反应条件
tin(IV) chloride in dichloromethane
T=-78°C; 0.5 h;
参考文献
Meanwell, Nicholas A.; Johnson, Carl R.
Synthesis, 1982 , # 4 p. 283 - 284
反应条件
titanium tetrachloride
参考文献
Cherkauskas, John P.; Cohen, Theodore
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 6 - 8
反应条件
titanium tetrachloride in dichloromethane
1.) -78 deg C, 1.5 h, 2.) -78 deg C to r.t.;
参考文献
Braga, Antonio L.; Dornelles, Luciano; Silveira, Claudio C.; Wessjohann, Ludger A.
Synthesis, 1999 , # 4 p. 562 - 564
反应条件
in nitromethane; dichloromethane
T=-78°C; 0.0833333 h;
参考文献
Reddy; Bellew; Prakash
Synthesis, 1992 , # 12 p. 1209 - 1210
反应条件
zinc(II) chloride in acetonitrile
T=20 - 25°C; 12 h; other solvents and times;
参考文献
Hatanaka, Kouhei; Tanimoto, Shigeo; Sugimoto, Toyonari; Okano, Masaya
Tetrahedron Letters, 1981 , vol. 22, # 34 p. 3243 - 3244
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=-30 - 20°C; 0.166667 h;
参考文献
Matsugi; Murata; Gotanda; Nambu; Anilkumar; Matsumoto; Kita
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2434 - 2441
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
0.166667 h; Yields of byproduct given;
参考文献
Matsugi, Masato; Gotanda, Kentoku; Murata, Kenji; Kita, Yasuyuki
Chemical Communications, 1997 , # 15 p. 1387 - 1388
反应条件
(i) LDA, THF, (ii) /BRN= 1696885/; Multistep reaction;
参考文献
Seebach,D.; Teschner,M.
Chemische Berichte, 1976 , vol. 109, p. 1601 - 1616
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=-30 - 20°C; 0.166667 h;
参考文献
Matsugi; Murata; Gotanda; Nambu; Anilkumar; Matsumoto; Kita
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2434 - 2441
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
T=-30 - 20°C; 0.166667 h;
参考文献
Matsugi; Murata; Gotanda; Nambu; Anilkumar; Matsumoto; Kita
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2434 - 2441
