1-(三甲基硅氧基)环戊烯合成路线 （共 155 条）
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
0.166667 h; Yields of byproduct given;
参考文献
Matsugi, Masato; Gotanda, Kentoku; Murata, Kenji; Kita, Yasuyuki
Chemical Communications, 1997 , # 15 p. 1387 - 1388
反应条件
trimethylsilyl trifluoromethanesulfonate in acetonitrile
0.166667 h; Yields of byproduct given;
参考文献
Matsugi, Masato; Gotanda, Kentoku; Murata, Kenji; Kita, Yasuyuki
Chemical Communications, 1997 , # 15 p. 1387 - 1388
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
a.) -78 deg C, 3 h; b.) r.t., 1 h;
参考文献
Wilson, Lawrence J.; Liotta, Dennis C.
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 1948 - 1950
反应条件
in dichloromethane
T=0°C; 15-30 min;
参考文献
Magnus, Philip; Rigollier, Pascal
Tetrahedron Letters, 1992 , vol. 33, # 41 p. 6111 - 6114
反应条件
tetrabutyl ammonium fluoride
T=-78°C; Substitution; Phenylsulfenylation;
参考文献
Tanaka; Azuma; Fang; Uchida; Iwata; Ishida; In; Maezaki
Synlett, 2000 , # 1 p. 33 - 36
反应条件
(i) LDA, THF, (ii) /BRN= 774156/; Multistep reaction;
参考文献
Seebach,D.; Teschner,M.
Chemische Berichte, 1976 , vol. 109, p. 1601 - 1616
反应条件
1: I2 / CH2Cl2
2: CH2Cl2
3: Et3N*HF / CH2Cl2 / 2 h
View Scheme
参考文献
Rubottom, George M.; Mott, Robert C.; Juve, Henrik D.
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2717 - 2721
反应条件
boron trifluoride diethyl etherate
1.) methylene dichloride, 20 deg C, 1 h; 2.) 1 h, 20 deg C; Yield given. Multistep reaction;
参考文献
Kashin, A. N.; Tul'chinskii, M. L.; Bumagin, N. A.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 8 p. 1390 - 1395
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1588 - 1595
反应条件
in dichloromethane
5 h; Ambient temperature;
参考文献
Rathore, Rajendra; Kochi, Jay K.
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 627 - 639
反应条件
titanium tetrachloride in dichloromethane
1.) -50 deg C 2.) room temperature, 2 h;
参考文献
Reetz, Manfred T.; Stephan, Wilfried
Liebigs Annalen der Chemie, 1980 , # 4 p. 533 - 541
