1-(三甲基硅氧基)环戊烯合成路线 (共 155 条)
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Journal of Organometallic Chemistry, , vol. 153, p. 137 - 151
反应条件
triethylamine in dichloromethane 0.25 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 31, # 6 p. 1619 - 1624
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature;
参考文献
Journal of Organometallic Chemistry, , vol. 185, # 2 p. 183 - 198
反应条件
trifluorormethanesulfonic acid; triethylamine 1) CH2Cl2, ice colling to r.t., 15 to 20 min, 2) CH2Cl2; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 5212 - 5214
反应条件
tetraphenyl stibonium bromide; N-phenyl-azilidine 1.) CH2Cl2, r.t., 5 min; 2.) 40 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Chemistry Letters, , p. 1247 - 1250
反应条件
pyrrolidin-2-one; tetraethylammonium tetrafluoroborate 1.) DME, HMPA, RT, electrochemical reduction, 2.) DME, HMPA, -75 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 493, # 1-2 p. 27 - 32
反应条件
sodium trimethyl-silanolate
参考文献
Chemische Berichte, , vol. 102, # 1 p. 14 - 22
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 48, # 8 p. 1738 - 1742,1587 - 1590
反应条件
triethylamine in 1,2-dichloro-ethane T=29°C; Rate constant;
参考文献
Liebigs Annalen der Chemie, , # 11 p. 1718 - 1721
反应条件
triethylamine in 1,2-dichloro-ethane T=27°C; Rate constant;
参考文献
Liebigs Annalen der Chemie, , # 11 p. 1718 - 1721