1: tetrahydrofuran; hexamethylphosphoric acid triamide / 3 h / 0 - 25 °C 2: KF / dimethylformamide / 0.5 h / 55 °C View Scheme
参考文献
Stefani, Helio A.; Cardoso, Lincoln D. G.; Valduga, Claudete J.; Zeni, Gilson
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 171-172, p. 167 - 172
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=0 - 25°C; 3 h;
参考文献
Stefani, Helio A.; Cardoso, Lincoln D. G.; Valduga, Claudete J.; Zeni, Gilson
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 171-172, p. 167 - 172
1.1: tetrahydrofuran; hexamethylphosphoric acid triamide / 3 h / 0 - 25 °C
2.1: KF / dimethylformamide / 0.5 h / 55 °C
3.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C
3.2: 100 percent / tetrahydrofuran
View Scheme
参考文献
Stefani, Helio A.; Cardoso, Lincoln D. G.; Valduga, Claudete J.; Zeni, Gilson
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 171-172, p. 167 - 172
1.1: tetrahydrofuran; hexamethylphosphoric acid triamide / 3 h / 0 - 25 °C
2.1: KF / dimethylformamide / 0.5 h / 55 °C
3.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C
3.2: 100 percent / tetrahydrofuran
View Scheme
参考文献
Stefani, Helio A.; Cardoso, Lincoln D. G.; Valduga, Claudete J.; Zeni, Gilson
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 171-172, p. 167 - 172
