1: in dichloromethane T=-78 - 20°C; 2 h; Inert atmosphere; 2: With methanol in dichloromethane T=-78 - 20°C; 0.5 h; Inert atmosphere; 3: With water in dichloromethane 1 h;
参考文献
Zervosen, Astrid; Bouillez, Andre; Herman, Alexandre; Amoroso, Ana; Joris, Bernard; Sauvage, Eric; Charlier, Paulette; Luxen, Andre
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 12 p. 3915 - 3924
