ammonia; KNH2

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oxalic acid in diethyl ether T=20°C; 1.5 h;

trichlorophosphate 1.) 30 deg C, 1 h, 2.) 20-30 deg C, 10 h; boiling water bath, 6h; Yield given. Multistep reaction;

1: 73 percent / p-toluenesulfonic acid / diethyl ether / 48 h / Ambient temperature 2: 98 percent / peroxybenzoic acid / CHCl3; diethyl ether / 20 h / 0 °C 3: 66 percent / lithium perchlorate / benzene / 4 h / Heating View Scheme

1: 73 percent / p-toluenesulfonic acid / diethyl ether / 48 h / Ambient temperature 2: 98 percent / peroxybenzoic acid / CHCl3; diethyl ether / 20 h / 0 °C 3: 66 percent / lithium perchlorate / benzene / 4 h / Heating 4: 89 percent / diethyl ether / 1.) -20 deg C, 15 min, 2.) -5 deg C, 4 h 5: potassium hydrogen sulfate / 0.17 h / 150 °C View Scheme

sulfuric acid

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