(S)-2-苯基-1-吡咯烷-1-甲基乙胺合成路线 （共 3 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 18 h; 2: With sodium hydroxide in tetrahydrofuran; water
参考文献
Infinity Discovery, Inc.
Patent: US2008/114167 A1, 2008 ;
Location in patent: Page/Page column 170 ;
US 20080114167 A1
反应条件
1: 99 percent / Et3N; (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium*PF6 / tetrahydrofuran / 8 h / 0 - 20 °C 2: AcCl; MeOH / 4 h / 0 - 20 °C 3: LiAlH4 / tetrahydrofuran / 48 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 30 p. 10504 - 10505
反应条件
1: AcCl; MeOH / 4 h / 0 - 20 °C 2: LiAlH4 / tetrahydrofuran / 48 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 30 p. 10504 - 10505
