di-tert-butyl peroxide; triethylsilane in further solvent(s) byproducts: 1-hexene, (C2H5)3SiOSi(C2H5)3; Irradiation (UV/VIS); at 180 K, degassed soln. of compd. in C3H6 was photolyzed with di-tert-butyl peroxide, in the EPR cavity by light from 500 W superpressure Hg arc lamp for 5 h; detected by GC-MS;

di-tert-butyl peroxide in further solvent(s) byproducts: 1-hexene; Irradiation (UV/VIS); at 180 K, degassed soln. of compd. in C3H6 was photolyzed with di-tert-butyl peroxide, in the EPR cavity by light from 500 W superpressure Hg arc lamp; chromy.;

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />&nbsp;addn. of BBr3 soln. to hexene soln. at -78&deg;C, slow warming to room temp., cooling to -10&deg;C, addn. of pinacol in Et2O, stirring 0.5h; addn. of Et2O, washing (H2O), drying, concn., distn.;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: BBr₃ / hexane / -78 - 20 &deg;C<br />2: hexane; diethyl ether / 0.5 h / -10 &deg;C<br /> <br /> &nbsp;